Organic Unknown Identification Report
Chemistry 266 Spring, 2007

40 points

Compound _________________________ Name __________________________

Unknown Number ___________________

Staple your IR spectrum, GC-MS, and ¹H and ¹³C NMR spectra to this report form.

1. Physical Examination

a. Physical state ________ b. Color ________ c. Odor ________

2. Physical Constants

a. M.P. _____________ b. B.P. ____________

3. Solubility Tests

H₂O _______, NaOH _______, NaHCO₃ ______, HCl ______, H₂SO₄ _______

In the following sections, more spaces are provided than may be necessary for your report. If there are not enough spaces, use the special comments section.

4. Spectra

Spectrum Type                     Peak (Characteristics)         Inferences
                                            (integration and multiplicity
                                            for NMR where appropriate)

a. ______________________________________________________________

b. ______________________________________________________________

c. ______________________________________________________________

d. ______________________________________________________________

e. ______________________________________________________________

f. ______________________________________________________________

g. ______________________________________________________________

h. ______________________________________________________________

i. ______________________________________________________________

j. ______________________________________________________________

k. ______________________________________________________________

l. ______________________________________________________________

m. ______________________________________________________________

n. ______________________________________________________________

o. ______________________________________________________________

p. ______________________________________________________________

q. ______________________________________________________________

r. ______________________________________________________________

s. ______________________________________________________________

t. ______________________________________________________________

u. ______________________________________________________________

v. ______________________________________________________________

w. ______________________________________________________________

x. ______________________________________________________________

y. ______________________________________________________________

z. ______________________________________________________________

5. Chemical Classification Tests:

            Reagent                             Results                                     Inferences

a. _______________________________________________________________

b. _______________________________________________________________

c. _______________________________________________________________

d. _______________________________________________________________

e. _______________________________________________________________

g. _______________________________________________________________

h. _______________________________________________________________

i. _______________________________________________________________

j. _______________________________________________________________

k. _______________________________________________________________

Functional Group(s) indicated by these tests _____________________